Bio-Analytical Chemistry

Bio-Analytical Chemistry

Bioanalytical Chemistry provides a thorough introduction for students and practitioners with a broad range of backgrounds from chemistry to medicine. In so doing, it brings together many of the techniques commonly used by biochemists and molecular biologists. The text includes entire chapters on design and implementation of enzyme assays; mass spectrometry; and validation of new methods. Each chapter progresses from basic concepts to applications involving real samples, and ends with a set of problems, while an appendix contains selected answers. The authors have limited mathematical derivations to those that are essential for an understanding of each method and they include a list of suggested reading for further information. This textbook provides an ideal companion for students, researchers, and industrial scientists working in chemistry, biology, biochemistry, pharmacy, and medicine.

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Encyclopedia of Analytical Chemistry: Applications, Theory and Instrumentation

Encyclopedia of Analytical Chemistry

Applications, Theory and Instrumentation

The new 3-Volume Supplementary Set for Encyclopedia of Analytical Chemistry contains 95 new articles (published online in Encyclopedia of Analytical Chemistry (EAC) from 2008 – 2010), covering subjects which have achieved particular prominence and distinction since the print publication of EAC in 2000. The new 3 Volume Set includes advances in applications and theory ranging from mass spectrometry, atomic, infrared, Raman and X-ray spectroscopy, to nuclear magnetic resonance and imaging, nuclear methods, electrochemistry, and hyphenated techniques.
Provides essential information required to analyze elements and compounds as well as structures in a wide variety of matrices for a range of applications, interpret the results and also gain a thorough knowledge of the theory and instrumentation utilized.

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Handbook of Acid-Base Indicators

Handbook of Acid-Base Indicators

While acid-base indicators continue to find new applications in an ever-widening range of scientific disciplines, there is no current book that focuses entirely on the subject, nor one that brings together the relevant advances that have evolved over the last three decades. The Handbook of Acid-Base Indicators compiles the most up-to-date, comprehensive information on over 200 water-based and solvent-based indicators into a single source.

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Dean's Analytical Chemistry Handbook

Dean's Analytical Chemistry Handbook

This comprehensive, up-to-date reference offers chemists and chemical engineers detailed coverage of the full range of analytical methods, including all conventional wet and instrumental techniques. It also provides information on the preliminary operations of analysis, preliminary separation methods, quality control and quality assurance, and statistics in chemical analysis.

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Pharmaceutical Analysis

Pharmaceutical Analysis

"Pharmaceutical Analysis: A Textbook for Pharmacy Students and Pharmaceutical Chemists" highlights the most important aspects of a wide range of techniques used in the control of the quality of pharmaceuticals, including spectroscopy, chromatography, and electrophoresis. This clear, practical guide also includes self-testing sections and arithmetical examples and tests to help students brush up on their arithmetical skills in an applied context.

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Introduction to Spectroscopy

Introduction to Spectroscopy

Gain an understanding of the latest advances in spectroscopy with the text that has set the unrivaled standard for more than 30 years: Pavia/Lampman/Kriz/Vyvyan's INTRODUCTION TO SPECTROSCOPY, 4e. This comprehensive resource provides an unmatched systematic introduction to spectra and basic theoretical concepts in spectroscopic methods that create a practical learning resource whether you're an introductory student or someone who needs a reliable reference text on spectroscopy. This well-rounded introduction features updated spectra; a modernized presentation of one-dimensional nuclear magnetic resonance (NMR) spectroscopy; the introduction of biological molecules in mass spectrometry; and inclusion of modern techniques alongside DEPT, COSY, and HECTOR. Count on this book's exceptional presentation to provide the comprehensive coverage you need to understand today's spectroscopic techniques.

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Spectrometric Identification of Organic Compounds

Spectrometric Identification of Organic Compounds

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Pharmaceutical Drug Analysis

Pharmaceutical Drug Analysis

‘Pharmaceutical Drug Analysis’ will prove to be a valuable and indispensable guide to
those working in Research & Development Laboratories, Quality Assurance Laboratories as well as Drug Testing Laboratories where either new products are being developed or routine analyses are carried out. Academicians and researchers engaged in the evaluation of pharmaceutical drug substances either in pure or dosage forms will also enormously benefit from ‘Pharmaceutical Drug Analysis’ by virtue of its ultimate goal of maintaining very high standards of quantitative analysis.
Finally, I wish to record here my special thanks to the numerous colleagues and friends who have not only extended their invaluable help by providing me with relevant sources of material but also by taking an active participation in the discussion of various chapters.
It is hoped that ‘Pharmaceutical Drug Analysis’ will soon prove to be an invaluable guide to both undergraduate and postgraduate students and to my esteemed colleagues in the teaching profession. Those working in Research & Development Laboratories, Quality Assurance Laboratories and Drug Testing laboratories will also find the book helpful in solving many of their intricate problems.


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Encyclopedia of Chromatography

Encyclopedia of Chromatography

A convenient source of information for workers in analytical chemistry, experimental biology, physics, and engineering, this second edition stands as is a clear guide to specific chromatographic techniques and principles. It provides a basic introduction to the science and technology of the method and covers an abundance of updated topics, applications, and key references to the recent literature. It includes over 400 cross-referenced articles with more than 80 entirely new articles and over 250 revisions, and many new discussions on emerging technologies and applications in chromatography. Numerous tables and figures illustrate technical points and applications presented in the text.


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Encyclopedia of Physical Science and Technology, Third Edition

Encyclopedia of Physical Science and Technology, Third Edition

ANALYTICAL CHEMISTRY is concerned with providing qualitative and quantitative information about the chemical and structural composition of a sample of matter. A huge variety of samples, from high concentrations of elements in alloy steels to part-per-billion levels of drugs in biological tissue, are handled by the analyst. The field is founded on the conversion of a measured physical property of the species being examined to a usable signal. It is generally divided into two categories, classical and instrumental, on the basis of its historical development. The overall strategy is to prepare a sample correctly, choose a particular method of analysis, and report the results in a meaningful format, which may include a statistical evaluation.

Although almost a decade has passed since the second edition of this work was published, this encyclopedia’s reputation as a high-quality scholarly work has not diminished. Guided by an advisory board comprising leading researchers (including eight Nobel laureates), editor in chief Meyers (Ramtech, Inc.) used a peer review process that produced over 780 articles written by experts. The coverage in this third edition has expanded to include molecular biology, biochemistry, and biotechnology. The decision to eliminate articles on military technology contributed to the deletion of about 200 articles; however, nearly 300 articles were added to cover new topics such as molecular electronics, nanostructured materials, tissue engineering, superstring theory, and the World Wide Web. The remaining articles were either updated or rewritten. Averaging 17-18 pages in length, the well-written articles present detailed information in a logical, organized manner. All follow a basic format: outline, glossary, defining statement, main body, cross references, and bibliography. A separate volume contains a list of contents by broad subject area, a relational index with groupings of connected articles, and the traditional subject index. The 20-volume McGraw-Hill Encyclopedia of Science & Technology (LJ 9/1/97) focuses on a broader range of scientific disciplines and a broader audience, so its articles are generally shorter and less detailed. With an intended audience of scientists and engineers and an emphasis on the physical sciences and technology, this encyclopedia aims to provide in-depth, authoritative coverage without limiting the mathematical treatment to algebra. This is an excellent source for students and researchers needing an overview of a particular subject. Highly recommended for academic and other types of libraries with significant science/technology collections.


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Organic Spectroscopic Analysis

Organic Spectroscopic Analysis

The aim of this textbook is not to provide you, the reader, with large numbers of correlation tables for every form of spectroscopy used by organic chemists; nor is it designed to give you an in-depth understanding of the physical processes that occur when molecules interact with electromagnetic radiation.

What authors hope to do in this textbook is to provide you with a basic understanding of how each type of spectroscopy gives rise to spectra, and how these spectra can be used to determine the structure of organic molecules. This text is aimed at undergraduate students in Years 1 and 2, and is meant to provide an introduction to organic spectroscopic analysis, leading to an appreciation of the information available from each form of spectroscopy and an ability to use spectroscopic information in the identification of organic compounds.

This book mainly concentrate upon the most commonly used techniques in organic structure determination: nuclear magnetic resonance (NMR), infrared (TR) and ultraviolet-visible (UV-Vis) spectroscopy, and mass spectrometry (MS). The amount of’ space devoted to each technique in this text is meant to be representative of their current usage for structure determination.

Finally, this book brings all of these techniques together in an attempt to show you how to go about the structure determination of an unknown compound in a (reasonably) logical manner. The main aim of this book has been to provide spectra to illustrate every point made, but do analyse fully each of the spectra in order to obtain the maximum information available.


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Handbook of Pharmaceutical Analysis by HPLC, Volume 6

Handbook of Pharmaceutical Analysis by HPLC, Volume 6

High pressure liquid chromatography frequently called high performance liquid chromatography (HPLC or, LC) is the premier analytical technique in pharmaceutical analysis and is predominantly used in the pharmaceutical industry. Written by selected experts in their respective fields, the Handbook of Pharmaceutical Analysis by HPLC Volume 6, provides a complete yet concise reference guide for utilizing the versatility of HPLC in drug development and quality control. Highlighting novel approaches in HPLC and the latest developments in hyphenated techniques, the book captures the essence of major pharmaceutical applications (assays, stability testing, impurity testing, dissolution testing, cleaning validation, high-throughput screening,

* A complete reference guide to HPLC
* Describes best practices in HPLC and offers 'tricks of the trade' in HPLC operation and method development
* Reviews key HPLC pharmaceutical applications and highlights currents trends in HPLC ancillary techniques, sample preparations, and data handling


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Analytical Instrumentation: Performance Characteristics and Quality

Analytical Instrumentation: Performance Characteristics and Quality

There is an increasing need for analysts to understand and be able to quantify the performance of analytical instruments, in particular with respect to the following:

* specifying equipment for purchase
* estimating uncertainties in intrumental measurements
* quantifying and demonstrating performance quality

This text links together an understanding of performance characteristics with an appreciation of the limitations imposed by instrument design, leading to the interplay of the validation and qualification processes within quality assurance systems.
A unique framework of topics covers the major instrumental techniques of spectrophotometry, chromatography, capillary electrophoresis, and atomic emission spectroscopy. The use of over 200 questions and answers, together with cross-referencing, helps to develop a thorough understanding of the various concepts that underpin the different techniques.
This book will appeal to a broad range of professional chemists, technicians and students, weither with reference to specific analytical techniques, or within a general course of study in instrumental performance. Analytical Techniques in the Sciences-This series of books provides coverage of all the major analytical techniques and their application in the most important areas of physical, life and materials sciences. Each text is presented in an open learning/distant learning style, in which the learning objectives are clearly identified. The reader's understanding of the material is constantly evaluated by the use of self-assessment and discussion questions.


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Analytical Gas Chromatography, Second Edition

Analytical Gas Chromatography, Second Edition

Gas chromatography remains the world's most widely used analytical technique, yet the expertise of a large proportion of chromatographers lies in other fields. Many users have little real knowledge of the variablesin the chromatographic process, the interaction between those variables, how they are best controlled, how the quality of their analytical results could be improved, and how analysis times can be shortened to facilitate the generation of a greater numberof more reliable results on the same equipment. An analyst with a more comprehensive understanding of chromatographic principles and practice, however, can often improve the quality of the data generated, reduce the analytical time, and forestall the needto purchase an additional chromatograph or another mass spectrometer.The Second Edition of Analytical Gas Chromatography is extensively revised with selected areas expanded and many new explanations and figures. The section on sample injection has been updated to include newer concepts of split, splitless, hot and cold on-column, programmed temperature vaporization, and large volume injections. Coverage of stationary phases now includes discussion, applications, and rationale of the increased thermal and oxidative resistance of the newly designed silarylenepolysiloxane polymers. Conventional and"extended range"polyethylene glycol stationary phases are examined from the viewpoints of temperature range and retention index reliabilities, and the chapter on"Variables"has been completely rewritten. The ways in which carrier gas velocity influences chromatographic performance is considered in detail, and includes what may be the first rational explanation of the seemingly anomalous effects that temperature exercises on gas viscosity (and gas flow). The practical effects that these changes cause to the chromatography is examined in pressure-, flow-, and"EPC-"regulated systems."Column Selection, Installation, and Use"has been completely rewritten as well. The accuracy of theVan Deemter plots has been greatly enhanced; a new program corrects for the first time for the changes in gas density and diffusion that occur during the chromatographic process because of solute progression through the pressure drop of the column. A new section has also been added on meeting thespecial requirements of columns destined for mass spectral analysis. The chapter on"Special Applications"has been expanded to include considerations of"selectivity tuning,"of fast analysis, and the section of Applications has been thoroughly updated and expanded.

Key Features:

* Incorporates nearly 60% new material
* Covers the newest concepts and materials for sample injection and stationary phases
* Presents detailed consideration of the influence of carrier gas velocity on practical aspects of chromatographic performance
* Contains a chapter on "Special Analytical Techniques" which includes consideration of selectivity tuning and fast analysis
* Provides a new section addressing the special requirements of columns to be used in mass spectral analysis
* Includes an improved program that greatly enhances the accuracy of the Van Deemter plots by more accurately depicting localized chromatographic conditions at each point in the column.


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Ion Exchange and Solvent Extraction: A Series of Advances, Volume 16

Ion Exchange and Solvent Extraction: A Series of Advances, Volume 16

Presenting key advancements in the areas of ion exchange and solvent extraction on par with the high-level research consistently related by this series, Volume 16 discusses the ion-exchange isothermal supersaturation technique, metal separation via pH-induced parametric pumping, modeling of ion-exchange kinetics for ultrapure water, ion-exchange properties of engineered carbons and carbonaceous materials, and many more topics.


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Handbook of Basic Tables for Chemical Analysis, Second Edition

Handbook of Basic Tables for Chemical Analysis, Second Edition

If you are a researcher in organic chemistry, chemical engineering, pharmaceutical science, forensics, or environmental science, you make routine use of chemical analysis. And like its best-selling predecessor was, the Handbook of Basic Tables for Chemical Analysis, Second Edition is your one-stop source for the information needed to design chemical analyses. Here's what is new in the Second Edition:"New chapters on solutions, electroanalytical methods, electrophoresis, and laboratory safety"An expanded section on gas chromatography that includes data on compounds that attack common detectors"New information on detector optimization"An updated section on high performance liquid chromatography that provides the most recent chiral stationary phases, detector information, and revised solvent tables"Updated information on the most useful "wet" chemistry methods"Enlarged section of Miscellaneous Tables Going far beyond the landmark first edition in terms of scope and applications, the second edition provides current and updated data culled from a wide range of resources and consolidated into a concise yet easy-to-use format. The book's laser-like focus on core information gives you the knowledge you need when you need it - at the decision point.


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Gas Chromatography in Biology and Medicine

Gas Chromatography in Biology and Medicine

IN the preface to the first edition of one of the earliest books on chromatography, Principles and Practice of Chromatography (Zechmeister and Cholnoky, 1943) there is written: “Every scientific advance is an advance in method.” It is also stated in this prefcice that “the invention of a new specialized laboratory procedure brings about rapid conquests in new fields of science and technology, finally it exhausts itself and is replaced by a still more practical method. The method of chromatographic adsorption invented by the talented Russian botanist, Professor M. Tswett makes possible spatial separation of components of a mixture. It is just now at the beginning of a bullish development : it offers a simple experimental procedure to the investigator especially in the fields of both pure and applied organic chemistry, of biochemistry and of physiology.”


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Methods for Structure Elucidation by High-Resolution NMR

Methods for Structure Elucidation by High-Resolution NMR

Nuclear Magnetic Resonance Spectroscopy (NMR) is now widely regarded as having evolved into a subscience. The field has become immensely diverse, ranging from medical use through solid state NMR to liquid state applications, with countless books and scientific journals devoted to these topics. Theoretical as well as experimental advance continues to be rapid, and has in fact accelerated by many novel innovations. This multi-authored book focuses on the latest developments in the rapidly evolving field of high resolution NMR, specifically with a view to applications on the structure elucidation of organic molecules of moderate molecular weight. Conceptually it differs from basic educational texts, hard-core scientific papers and regular review articles in that each chapter may be regarded as the authors' personal account of their special insights and results that crystallised after several years of research into a given topic. The book revolves around several themes and offers a handful of scientific "gems" of various colors, reflecting the great diversity of NMR. It contains 16 loosely connected chapters written by some of today's most accomplished NMR scientists in the world. Each chapter is a unique synthesis of the authors' previous research results in the given field, and thus projects special insights. Much emphasis has been given to the latest developments in NMR, in particular to selective pulses and pulsed field gradients. As a part of the series "Analytical Spectroscopy Library", with subsequent editions coming along this book should provide a platform for future research accounts of similar flavor. The material is presented in a mostly non-mathematical fashion, and is intended mainly for chemists, application NMR scientists and students with already some background in NMR. Some of the chapters slightly overlap in the discussed topics, which is particularly exciting in terms of gaining insight into the same area from different angles.


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Structure Elucidation by NMR in Organic Chemistry

Structure Elucidation by NMR in Organic Chemistry
Publisher: Wiley | 3 edition (December 3, 2002) | ISBN: 0470850078 | Pages: 270 | PDF | 8.7 MB

This text provides the graduate student with a systematic guide to unravelling structural information from the NMR spectra of unknown synthetic and natural compounds. A brief introduction gives an overview of the basic principles and elementary instrumental methods of NMR. This is followed by instructional strategy and tactical advice on how to translate spectra into meaningful structural information. The book provides the student with 55 sets of spectra of graduated complexity. These are designed to challenge the student's problem-solving abilities by the introduction of new concepts with each group of problems, followed by possible solutions and full explanations. A formula index of solutions is provided at the end of the text. This third edition, following on from the second (a reprint of the first edition with corrections), presents significant new material. Thus, actual methods of two-dimensional NMR such as some inverse techniques of heteronuclear shift correlation, as well as the detection of proton-proton connectivities and nuclear Overhauser effects are included. To demonstrate the applications of these methods, new problems have replaced those of previous editions.


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Bioanalytical Separations, Volume 4

Bioanalytical Separations, Volume 4

Bioanalytical Separations is volume 4 of the multi-volume series, Handbook of Analytical Separations, providing reviews of analytical separation methods and techniques used for the determination of analytes across a whole range of applications. The theme for this volume is bioanalysis, in this case specifically meaning the analysis of drugs and their metabolites in biological fluids.

- Discusses new developments in instrumentation and methods of analyzing drugs and their metabolites in biological fluids
- Provides guidance to the different methods, their relative value to the user, and the advantages and pitfalls of their use
- Future trends are identified, in terms of the potential impact of new technologies.


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